Abstract
Ten cycloketone 2,4-dinitrophenylhydrazones have been chromatographed by thin-layer techniques using Eastman Chromagram sheets coated with silica gel and developed with benzene in Eastman sandwich apparatus. Good separations of all test compounds from binary mixtures with the standard cyclohexanone 2,4-dinitrophenylhydrazone are reported as well as good separations of more complex mixtures of the test compounds. Lack of precision is noted despite a rigorous standardized procedure. Evidence is offered that chromagram sheets differ in adsorbent activity.
Library of Congress Subject Headings
Thin layer chromatography; Chemistry, Analytic
Publication Date
6-1-1968
Document Type
Thesis
Department, Program, or Center
School of Chemistry and Materials Science (COS)
Advisor
Gilman, Robert
Recommended Citation
Slentz, Robert, "Thin-layer chromatographic separations of cycloketone 2,4-dinitrophenylhydrazones" (1968). Thesis. Rochester Institute of Technology. Accessed from
https://repository.rit.edu/theses/3717
Campus
RIT – Main Campus
Comments
Note: imported from RIT’s Digital Media Library running on DSpace to RIT Scholar Works. Physical copy available through RIT's The Wallace Library at: QD117.C5 S55